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Carbon 2011, Vol. 49 (10) :3184 -3189 doi:10.1016/j.carbon.2011.03.042 <<-上一篇 下一篇 ->>
Preparation of ordered mesoporous carbon membranes by a soft-templating;method
Tanaka, Shunsuke;Nakatani, Norihito;Doi, Anna;Miyake, Yoshikazu
[Tanaka, Shunsuke; Nakatani, Norihito; Doi, Anna; Miyake, Yoshikazu] Kansai Univ, Fac Environm & Urban Engn, Dept Chem Energy & Environm Engn, Suita, Osaka 5648680, Japan.;[Tanaka, Shunsuke; Miyake, Yoshikazu] Kansai Univ, High Technol Res Ctr, Suita, Osaka 5648680, Japan.
Abstract: Preparation of continuous mesoporous carbon membranes without the use of an intermediate inorganic template was achieved using a thermosetting phenolic resin, resorcinol/phloroglucinol/formaldehyde, and a thermally-decomposable organic template, Pluronic F127 (PEO(106)-PPO(70)-PEO(106)). The coating solution was cast on porous alpha-alumina supports by dip-coating. Afterwards, decomposition of the organic template and solidification of the carbon precursors are simultaneously performed through a carbonization process. A composite layer of carbon/alumina was formed. The single gas permeation was governed by the Knudsen diffusion mechanism. The membrane exhibited high hydrothermal stability and high alkaline resistance. (C) 2011 Elsevier Ltd. All rights reserved.
收稿日期:2 February 2011     发布日期: 31 March 2011    
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